HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Methanesulfonamidophenyl)boronic acid → HCID 67447346, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Methanesulfonamidophenyl)boronic acid | HCID 2773537 | — |
| Reactant | 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one | HCID 67449139 | — |
| Product | HCID 67447346 | HCID 67447346 | 99.9% |
Reaction Steps
Following Step 1 from General Procedure B, 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one (50 mg, 0.10 mmol) was reacted with 4-(methylsulfonamido)phenylboronic acid (52 mg, 0.24 mmol) to afford the desired product (40 mg, 62%) as a brown solid: ESI MS m/z 400 [C19H16N2O4S2+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962648B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-57c1cf23433848eca57566a7fab73912 |
| Source note | uspto-grants-2015_02 |