HuagongsheHuagongshe Chemistry Print Report · For research reference only
Borane → HCID 67447585, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Borane | HCID 6331 | — |
| Reactant | HCID 67447554 | HCID 67447554 | — |
| Product | HCID 67447585 | HCID 67447585 | 60% |
Reaction Steps
Following the procedure outlined for Example 265, 3-[4-(8-methoxy-4-oxo-4,5-dihydrothieno[2,3-c]quinolin-9-yl)phenyl]propanenitrile (250 mg, 0.69 mmol) was reacted with borane (1.0 M in THF, 10 mL, 10 mmol) to afford the desired product (150 mg, 60%) as a brown oil: ESI MS m/z 365 [C21H20N2O2S+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962648B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-1c7ec7cf08fb457aaba766bb73efb95a |
| Source note | uspto-grants-2015_02 |