huagongshe.com
HRID1853784

反应详情

EQUATION

反应方程式

HRID 1853784 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc2[nH]c(=O)c3sccc3c2c1Br
HCID67449139

未命名化合物

结构：C[C@H](NC(=O)OC(C)(C)C)c1ccc(B2OC(C)(C)C(C)(C)O2)cc1
HCID67451913

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2[nH]c(=O)c3sccc3c2c1-c1ccc([C@H](C)NC(=O)OC(C)(C)C)cc1
HCID86689487

未命名化合物

收率 67.5%

PROCEDURE

实验过程

Following General Procedure B, 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one (760 mg, 2.4 mmol) was reacted with (S)-tert-butyl 1-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]ethylcarbamate (1.3 g, 3.7 mmol) to afford the desired product (730 mg, 66%) as a light yellow solid: ESI MS m/z 451 [C25H26N2O4S+H]+.