HuagongsheHuagongshe Chemistry Print Report · For research reference only
B-[4-[1-(Dimethylamino)ethyl]phenyl]boronic acid → HCID 67448087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | B-[4-[1-(Dimethylamino)ethyl]phenyl]boronic acid | HCID 45791080 | — |
| Reactant | 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one | HCID 67449139 | — |
| Product | HCID 67448087 | HCID 67448087 | 60.5% |
Reaction Steps
Following General Procedure B, 9-bromo-8-methoxythieno[2,3-c]quinolin-4(5H)-one (1.5 g, 4.8 mmol) was reacted with 4-[1-(dimethylamino)ethyl]phenylboronic acid (1.5 g, 6.3 mmol) to afford the desired product (1.1 g, 58%) as a white solid: ESI MS m/z 379 [C22H22N2O2S+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962648B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-797896f0420f4b778076a4187fd508bd |
| Source note | uspto-grants-2015_02 |