HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 86689498, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 67447234 | HCID 67447234 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86689498 | HCID 86689498 | 51% |
Reaction Steps
Following General Procedure I, tert-butyl 4-(8-methoxy-4-oxo-4,5-dihydrothieno[2,3-c]quinolin-9-yl)benzylcarbamate (0.66 g, 1.5 mmol) was reacted with N-bromosuccinimide (0.30 g, 1.7 mmol) in DMF (10 mL) to afford the desired product (0.39 g, 51%) as a brown solid: ESI MS m/z 515 [C24H23BrN2O4S+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962648B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-bdd6f5f964394af69a428bcece3fa176 |
| Source note | uspto-grants-2015_02 |