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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1853815Generated: November 2, 2026

N-bromobutanimide → HCID 86689498, compound

https://huagongshe.com/reaction/1853815

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN-bromobutanimideHCID 67184—
ReactantHCID 67447234HCID 67447234—
SolventDimethylformamideHCID 6228—
ProductHCID 86689498HCID 8668949851%

Reaction Steps

Following General Procedure I, tert-butyl 4-(8-methoxy-4-oxo-4,5-dihydrothieno[2,3-c]quinolin-9-yl)benzylcarbamate (0.66 g, 1.5 mmol) was reacted with N-bromosuccinimide (0.30 g, 1.7 mmol) in DMF (10 mL) to afford the desired product (0.39 g, 51%) as a brown solid: ESI MS m/z 515 [C24H23BrN2O4S+H]+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08962648B2
Source datasetuspto-grants-2015_02
ORD IDord-bdd6f5f964394af69a428bcece3fa176
Source noteuspto-grants-2015_02