HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylboroxine → HCID 67449497, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylboroxine | HCID 574072 | — |
| Reactant | HCID 86689498 | HCID 86689498 | — |
| Product | HCID 67449497 | HCID 67449497 | 95.4% |
Reaction Steps
Following General Procedure J, tert-butyl 4-(6-bromo-8-methoxy-4-oxo-4,5-dihydrothieno[2,3-c]quinolin-9-yl)benzylcarbamate (52 mg, 0.10 mmol) was reacted with trimethylboroxine (13 mg, 0.10 mmol) to afford the desired product (43 mg, 95%) as a grey solid: ESI MS m/z 451 [C25H26N2O4S+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962648B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-e2ad45b839ce4818b5a43b36a7d76d79 |
| Source note | uspto-grants-2015_02 |