HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 67450402, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 67448984 | HCID 67448984 | — |
| Product | HCID 67450402 | HCID 67450402 | 28% |
Reaction Steps
Following General Procedure F, 1-[4-(8-methoxy-4-oxo-4,5-dihydrothieno[2,3-c]quinolin-9-yl)phenyl]cyclopropanecarbonitrile (340 mg, 0.91 mmol) was reacted with tribromoborane (1.3 mL) to afford the desired product (90 mg, 28%) as a light brown solid: ESI MS m/z 359 [C21H14N2O2S+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962648B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-2cec37664cc546b4976ed7e94262f957 |
| Source note | uspto-grants-2015_02 |