HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → N-Ethyl-4-bromobenzylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | 4-Bromobenzyl bromide | HCID 68527 | — |
| Product | N-Ethyl-4-bromobenzylamine | HCID 4716477 | 75.9% |
Reaction Steps
Following the procedure outlined for Example 488, 1-bromo-4-(bromomethyl)benzene (2.0 g, 8.0 mmol) was reacted with ethanamine (720 mg, 16 mmol) to afford the desired product (1.3 g, 75%) as a brown solid: ESI MS m/z 215 [C9H12BrN+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962648B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-1a26f87c973348ab9dc589b9c4020042 |
| Source note | uspto-grants-2015_02 |