(2-Methoxyethyl)(methyl)amine → HCID 67324786, compound

Participants

Reaction Steps

Prepared as for 5-[6-(4-methylpyridin-2-ylamino)pyridin-2-yl]-*(pyridin-4-ylmethyl)-oxazol-2-amine above from 3-(2-chloro-oxazol-5-yl)-5-(4-methyl-pyridin-2-ylamino)-benzonitrile and N-(2-methoxyethyl)methylamine in iPrOH. (400 MHz, DMSO-d6) δ 9.38 (s, 1H), 8.18 (d, J=1.7 Hz, 1H), 8.10 (d, J=5.1 Hz, 1H), 7.87 (t, J=1.7 Hz, 1H), 7.49 (t, J=1.4 Hz, 1H), 7.41 (s, 1H), 6.70 (d, J=5.3 Hz, 1H), 6.68 (s, 1H), 3.64-3.60 (m, 2H), 3.60-3.55 (m, 2H), 3.29 (s, 3H), 3.11 (s, 3H), 2.26 (s, 3H) (ESI+) m/z 364 (M+H)+. Retention time=2.55 mins (method 1).

Provenance & Evidence