HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 44538540, compound → HCID 67106833, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 44538540 | HCID 44538540 | — |
| Reactant | HCID 67107578 | HCID 67107578 | — |
| Product | HCID 67106833 | HCID 67106833 | — |
Reaction Steps
The title compound was synthesized using the same procedure employed for Example 349, but with (1E,6E)-1-(5-benzyloxy-2-nitrophenyl)-7-(4-hydroxyphenyl)hepta-1,6-diene-3,5-dione (10 mg, 22 μmol, synthesized in Example 342) as the starting material instead of (1E,6E)-1-(4-hydroxyphenyl)-7-(2-nitrophenyl)hepta-1,6-diene-3,5-dione, and was purified by silica gel column chromatography eluting with hexane/ethyl acetate=75/25 to 60/40. The product was obtained as a solid (3.3 mg, 35%) having the following characteristics.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962674B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-d5371539b12d49c6a6d02c6316da11b6 |
| Source note | uspto-grants-2015_02 |