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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1854699Generated: October 31, 2026

HCID 44538540, compound → HCID 67106833, compound

https://huagongshe.com/reaction/1854699

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 44538540HCID 44538540—
ReactantHCID 67107578HCID 67107578—
ProductHCID 67106833HCID 67106833—

Reaction Steps

The title compound was synthesized using the same procedure employed for Example 349, but with (1E,6E)-1-(5-benzyloxy-2-nitrophenyl)-7-(4-hydroxyphenyl)hepta-1,6-diene-3,5-dione (10 mg, 22 μmol, synthesized in Example 342) as the starting material instead of (1E,6E)-1-(4-hydroxyphenyl)-7-(2-nitrophenyl)hepta-1,6-diene-3,5-dione, and was purified by silica gel column chromatography eluting with hexane/ethyl acetate=75/25 to 60/40. The product was obtained as a solid (3.3 mg, 35%) having the following characteristics.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08962674B2
Source datasetuspto-grants-2015_02
ORD IDord-d5371539b12d49c6a6d02c6316da11b6
Source noteuspto-grants-2015_02