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HRID1854813

反应详情

EQUATION

反应方程式

HRID 1854813 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)c1cc(F)ccc1C(F)(F)F
HCID2737560

5-Fluoro-2-(trifluoromethyl)benzoyl chloride

C8H3ClF4O

结构：c1cnc(N2CCNCC2)nn1
HCID12296696

未命名化合物

PRODUCTS

生成物

2
结构：O=C(c1ccccc1C(F)(F)F)N1CCN(c2nccnn2)CC1
HCID53493384

未命名化合物

收率 67%
结构：O=C(c1cc(F)ccc1C(F)(F)F)N1CCN(c2nccnn2)CC1
HCID53493507

未命名化合物

PROCEDURE

实验过程

Compound 4 is prepared from 5-fluoro-2-trifluoromethyl-benzoyl chloride and intermediate 5a according to synthesis method 2 under the operating conditions described for example 3 (67% yield).

WORKUP

后处理

  1. customaccording to synthesis method 2 under the operating conditions