2,5-Dichlorophenol → HCID 53494179, compound

HRID 1854816Notes

Reaction equation

HRID 1854816 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([Cl:8])=[CH:4][C:3]=1[OH:9].[CH3:10][CH:11]1[CH:16](O)[CH2:15][CH2:14][N:13]([C:18]2[N:19]=[N:20][CH:21]=[CH:22][N:23]=2)[CH2:12]1>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([Cl:8])=[CH:4][C:3]=1[O:9][CH:16]1[CH2:15][CH2:14][N:13]([C:18]2[N:19]=[N:20][CH:21]=[CH:22][N:23]=2)[CH2:12][CH:11]1[CH3:10]

Participants

3

Reactant 2

HCID 662,5-DichlorophenolHCID 86676670HCID 86676670, compound

Product 1

HCID 53494179HCID 53494179, compound

Procedure

Compound 38 is prepared from 2,5-dichlorophenol and intermediate 5c according to synthesis method 3 under the operating conditions described for example 8 (37% yield).

Workup

  1. customaccording to synthesis method 3 under the operating conditions

Sources & evidence

ORD record
ord-a459367b7edd44739d6690556f8f25ed
Source dataset
uspto-grants-2015_02
Patent number
US08962837B2

Reaction notes

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