Allyl bromide → HCID 90315174, compound

HRID 1855205Notes

Reaction equation

[C:1]([C:3]1[S:4][C:5]2[CH:11]=[C:10]([OH:12])[CH:9]=[CH:8][C:6]=2[N:7]=1)#[N:2].[CH2:13](Br)[CH:14]=[CH2:15]>>[CH2:15]([O:12][C:10]1[CH:9]=[CH:8][C:6]2[N:7]=[C:3]([C:1]#[N:2])[S:4][C:5]=2[CH:11]=1)[CH:14]=[CH2:13]

Participants

Reactant 2

HCID 7841Allyl bromide

HCID 98819122-Cyano-6-hydroxybenzothiazole

Product 1

HCID 90315174HCID 90315174, compound

Procedure

In greater detail, 2-cyano-6-methoxybenzothiazole is used as a starting material and reacted with pyridine hydrochloride to yield 2-cyano-6-hydroxybenzothiazole. Next, the 2-cyano-6-hydroxybenzothiazole is reacted with allyl bromide to yield 6-allyloxy-benzothiazole-2-carbonitrile.

Sources & evidence

ORD record: ord-de487a7e1ef549adb5730d167e3dc44c
Source dataset: uspto-grants-2015_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08962854B2

Reaction notes

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