Imidazole → HCID 11383144, compound

Participants

Reaction Steps

To a flask containing (S)-1-(4-Bromo-phenyl)-hexan-1-ol in CH2Cl2 at ambient temperature (˜23° C.) was added imidazole and t-butyldimethylsilyl chloride. The reaction mixture was stirred at ambient temperature for a period of time until all starting material was consumed before quenching with a mixture of MeOH and water. The organic layer was washed with deionized water and concentrated under reduced pressure to give the product as a yellow oil.

Provenance & Evidence