1-(Bromomethyl)-3-chlorobenzene → HCID 86633615, compound

HRID 1855328Notes

Reaction equation

HRID 1855328 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][CH:9]=1)[CH2:5]Br.[Cl:10][C:11]1[N:16]=[C:15](Cl)[CH:14]=[C:13]([Cl:18])[N:12]=1>>[Cl:10][C:11]1[N:12]=[C:13]([Cl:18])[CH:14]=[C:15]([CH2:5][C:4]2[CH:7]=[CH:8][CH:9]=[C:2]([Cl:1])[CH:3]=2)[N:16]=1

Participants

3

Reactant 2

HCID 698381-(Bromomethyl)-3-chlorobenzeneHCID 773782,4,6-Trichloropyrimidine

Product 1

HCID 86633615HCID 86633615, compoundYield 26%

Procedure

The title compound was prepared in analogous manner as described in example 2a) from 3-chloro-benzylbromide and 2,4,6-trichloropyrimidine. It was obtained as a pale-yellow oil in 26% yield.

Workup

  1. customIt was obtained as a pale-yellow oil in 26% yield

Sources & evidence

ORD record
ord-edc8dc8400374ee2abf954f509ff02a9
Source dataset
uspto-grants-2015_02
Patent number
US08962834B2

Reaction notes

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