HCID 68631010, compound → HCID 57829756, compound

HRID 1855368Notes

Reaction equation

HRID 1855368 reaction equation
[CH2:1]([O:3][C:4](=[O:25])[CH:5]([C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1)[C:6](=O)[C:7]([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)=[CH:8]N(C)C)[CH3:2].[N+]([O-])(O)=O.[N+]([O-])(O)=O.[CH3:34][O:35][C:36]1[CH:37]=[C:38]([NH:48][C:49]([NH2:51])=[NH:50])[CH:39]=[CH:40][C:41]=1[N:42]1[CH:46]=[C:45]([CH3:47])[N:44]=[CH:43]1>>[CH3:34][O:35][C:36]1[CH:37]=[C:38]([NH:48][C:49]2[N:51]=[C:6]([CH:5]([C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[C:4]([O:3][CH2:1][CH3:2])=[O:25])[C:7]([C:12]3[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=3)=[CH:8][N:50]=2)[CH:39]=[CH:40][C:41]=1[N:42]1[CH:46]=[C:45]([CH3:47])[N:44]=[CH:43]1

Participants

3

Reactant 2

HCID 68631010HCID 68631010, compoundHCID 178493228HCID 178493228, compound

Product 1

HCID 57829756HCID 57829756, compound

Procedure

The title compound was prepared from ethyl-5-dimethylamino-3-oxo-2,4-diphenyl-pent-4-enoate (102 mg, 0.3 mmol) and N-[3-methoxy-4-(4-methyl-imidazol-1-yl)-phenyl]-guanidine dinitrate (83 mg, 0.22 mmol) using in analogous manner the procedure described in example 28b). Obtained as a light-brown solid (5 mg, 3%). Mp 84-86° C.

Sources & evidence

ORD record
ord-b1294d40af7d4ab98f7ad010190fd77e
Source dataset
uspto-grants-2015_02
Patent number
US08962834B2

Reaction notes

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