HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-benzyl-4,6-dichloropyrimidine → HCID 44192796, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-benzyl-4,6-dichloropyrimidine | HCID 2775259 | — |
| Reactant | 3-methoxy-4-(4-methyl-1H-imidazol-1-yl)aniline | HCID 45480181 | — |
| Product | HCID 44192796 | HCID 44192796 | 48% |
Reaction Steps
The title compound was prepared in analogous manner as described in example 62 from 2-benzyl-4,6-dichloro-pyrimidine and 3-methoxy-4-(4-methyl-imidazol-1-yl)-phenylamine. Obtained as yellow solid in 48% yield after column chromatography of the crude product on silica gel using dichloromethane/methanol (98:2 and then 95:5 v/v) as eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962834B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-70688ba1734d47fbb5ff4374e3542585 |
| Source note | uspto-grants-2015_02 |