HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-methoxy-4-(4-methyl-1H-imidazol-1-yl)aniline → HCID 57829773, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-methoxy-4-(4-methyl-1H-imidazol-1-yl)aniline | HCID 45480181 | — |
| Reactant | HCID 86633622 | HCID 86633622 | — |
| Product | HCID 57829773 | HCID 57829773 | 13% |
Reaction Steps
Prepared in analogy to example 81b) from 3-methoxy-4-(4-methyl-imidazol-1-yl)-phenylamine and 2-chloro-4-methyl-6-(4-trifluoromethoxy-phenoxy)-pyrimidine in a yield of 13%. MS ISP (m/e): 472.1 (100) [(M+H)+]. 1H NMR (CDCl3, 300 MHz): δ (ppm)=7.44 (s, 1H), 7.35-7.15 (m, 5H), 7.01 (s, 2H), 6.86 (s, 1H), 6.30 (s, 1H), 3.63 (s, 3H), 2.43 (s, 3H), 2.39 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962834B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-17c9e6f10e744d85909dac2df3af9354 |
| Source note | uspto-grants-2015_02 |