2,6-Dichloropyridine → HCID 86633629, compound

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Reaction Steps

Prepared in analogy to example 62 from 3-methoxy-4-(4-methyl-imidazol-1-yl)-phenylamine and 2,6-dichloropyridine. The title compound was obtained as a yellow solid (Yield=60%). MS ISP (m/e): 315.1 & 317.1 (100 & 37) [(M+H)+]. 1H NMR (CDCl3, 300 MHz): 8 (ppm)=7.63 (s, 1H), 7.48 (t, 1H), 7.37 (s, 1H), 7.18 (d, 1H), 6.95-6.80 (m, 2H), 6.82 (d, 1H), 6.72 (d, 1H), 6.64 (s, 1H), 3.86 (s, 3H), 2.30 (s, 3H).

Provenance & Evidence