HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 528635, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | N-tert-Butylpivalamide | HCID 299326 | — |
| Product | HCID 528635 | HCID 528635 | 96% |
Reaction Steps
In a fashion similar to the preparation of LtBu,tBuH, treatment of isopropylamine (9.0 mL, 105 mmol) and triethylamine (14.9 mL, 105 mmol) with pivaloyl chloride (8.9 mL, 100 mmol) afforded LtBu,iPrH as white crystalline solid (13.75 g, 96%) upon sublimation at 55° C./0.05 Torr: mp 106-108° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962876B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-37851dbe5a584ace904b771f16bdcc4e |
| Source note | uspto-grants-2015_02 |