HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 56921332, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | 3-Pentanamine, 2,4-dimethyl- | HCID 77702 | — |
| Reactant | N-tert-Butylpivalamide | HCID 299326 | — |
| Product | HCID 56921332 | HCID 56921332 | 98% |
Reaction Steps
In a fashion similar to the preparation of LtBu,tBuH, treatment of 2,4-dimethylpentan-3-amine (14.0 mL, 100 mmol) and triethylamine (14.9 mL, 105 mmol) with pivaloyl chloride (8.9 mL, 100 mmol) afforded LtBu,CHiPr2H as white crystalline solid (19.53 g, 98%) upon sublimation at 65° C./0.05 Torr: mp 107-109° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08962876B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-e70af365870f41f0b6a905ee58549251 |
| Source note | uspto-grants-2015_02 |