HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 4-(p-Allyloxyphenyl)-2-butanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4-(4'-Hydroxyphenyl)-2-butanone | HCID 21648 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-(p-Allyloxyphenyl)-2-butanone | HCID 24708775 | — |
Reaction Steps
p-Hydroxy benzylacetone (1.5 g.), KOH (6 g.) and allyl bromide (1.2 g.) were stirred in ethanol (50 ml) overnight. Water was added and the mixture extracted with ether, which was evaporated to give the compound (1.6 g.) as an oil purified by column chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04216232 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-84efceb907c94cf0a2755f19e0d3115b |
| Source note | uspto-grants-1980_08 |