HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 3-(4-Bromophenyl)-N,N-dimethyl-3-(pyridin-3-yl)prop-2-en-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | HCID 53820556 | HCID 53820556 | — |
| Product | 3-(4-Bromophenyl)-N,N-dimethyl-3-(pyridin-3-yl)prop-2-en-1-amine | HCID 41987 | — |
Reaction Steps
The brown solution of the chloride from step 3 (from 0.1 moles ketone) in ca 160 ml of solvent was stirred at ca 0° C. and 26 g dimethylamine were added in one portion. This solution was stirred at 0°-5° C. for 2 hours. The solvent was then evaporated. A crude brown oil of the desired end product was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04216328 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-584dd569088f4c35abc7b9aef6f17d00 |
| Source note | uspto-grants-1980_08 |