HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 12878607, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Glycinamide hydrochloride | HCID 2723639 | — |
| Reactant | 2-[3-(Dimethylamino)propoxy]benzaldehyde | HCID 2995968 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12878607 | HCID 12878607 | 93.9% |
Reaction Steps
Fifteen grams of 2-(3-dimethylaminopropoxy)benzaldehyde and 8.1 g of glycinamide, hydrochloride are reacted in 300 ml of ethanol in the presence of 4.8 g of 85% potassium hydroxide as described in Example 1 to give 20 g of a crude semi-solid product. The crude product is triturated with 100 ml of isopropyl ether and cooled to yield 17.9 g of solid; melting point 71°-73° C. (sintering at 60° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04216335 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-b625b464f49d47109c4d5ef9c1d32263 |
| Source note | uspto-grants-1980_08 |