HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Pyridylmethyl-2-methylthio-4-pyrimidone → HCID 14338594, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Pyridylmethyl-2-methylthio-4-pyrimidone | HCID 12783823 | — |
| Reactant | 3-[(4-methyl-1H-imidazol-5-yl)methylthio]propylamine | HCID 13520576 | — |
| Product | HCID 14338594 | HCID 14338594 | — |
Reaction Steps
An intimate mixture of 5-(3-pyridylmethyl)-2-methylthio-4-pyrimidone and 3-(5-methyl-4-imidazolylmethylthio)propylamine is heated at 130°-135° for 7 hours. The cool mixture is triturated with hot water and treated with dilute ethanolic HCl to give the trihydrochloride of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04216318 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-2477ff17ed70466aa5290a08adc44b8c |
| Source note | uspto-grants-1980_08 |