HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oct-2-ene → Methyl-undec-9-enoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oct-2-ene | HCID 8126 | — |
| Reactant | Methyl Oleate | HCID 5364509 | — |
| Product | Methyl-undec-9-enoate | HCID 62588 | 5% |
Reaction Steps
Reaction was carried out in the same manner as in Example 1, except that a mixture of 1 ml of methyl oleate and 1 ml of 2-octene was used in place of 1 ml of the methyl oleate, the reaction temperature was 70° C., and the reaction time was 17 hours. There were obtained methyl 9-undecenoate in a yield of about 5% and methyl 9-pentadecanoate in a yield of about 7% (estimated from the chromatogram). Besides, metathesis products were obtained independently from methyl oleate and 2-octene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04217299 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-2dd0dc184fc1498498593a91c8adadba |
| Source note | uspto-grants-1980_08 |