HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylamine → HCID 23346042, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylamine | HCID 7912 | — |
| Reactant | m-Phenylenediisothiocyanate | HCID 18404 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 23346042 | HCID 23346042 | — |
Reaction Steps
To a solution of 3.84 g. of 1,3-phenylenediisothiocyanate in 100ml. of acetonitrile is added 4.4 g. of diisopropylamine and the mixture is refluxed for 3 hours. The solvent is removed in vacuo and the residue is crystallized from acetonitrile to yield 3.5 g. of the title compound, melting point 128°-129° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04218396 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-1c4dea560d034cffa175af3d269fd68e |
| Source note | uspto-grants-1980_08 |