HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23346235, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Aluminiumhydride | HCID 21584524 | — |
| Reactant | HCID 23346234 | HCID 23346234 | — |
| Reactant | HCID 23346262 | HCID 23346262 | — |
| Product | HCID 23346235 | HCID 23346235 | 83.1% |
Reaction Steps
According to the procedure for synthesis of 4-(phenylthio)-1,2,3,6-tetrahydropyridine, 58.5 g of 4-[(4-fluorophenyl)thio]pyridine is reduced with aluminum hydride. The crude oil is treated with ethereal hydrogen chloride to give 58.2 g (83.1%) of white powder, m.p. 136°-142° C. Recrystallization from acetonitrile gives white crystals, m.p. 158°-159° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04218455 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-44692acce0db4d80867cfb3868ecef14 |
| Source note | uspto-grants-1980_08 |