HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → N-(3-chloro-2-methylphenyl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 3-Chloro-2-methylaniline | HCID 6894 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-(3-chloro-2-methylphenyl)acetamide | HCID 81969 | — |
Reaction Steps
141 g. of 3-chloro-2-methylaniline (1 mol.) was added to a stirred mixture of 200 ml. of acetic acid and 102 g. (1 mol.) of acetic anhydride and heated to 95° C. for approximately one hour. The mixture was poured into water and filtered to give 3-chloro-2-methylacetanilide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04218464 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-bbda59e7845b4ffe95493ff3f671d42c |
| Source note | uspto-grants-1980_08 |