Isomescaline → HCID 23346555, compound

HRID 1856249Notes

Reaction equation

HRID 1856249 reaction equation
[OH2:1].[CH2:2]([O:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[C:16]([CH:18]=O)=O)[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[CH3:20][O:21][C:22]1[C:30]([O:31][CH3:32])=[C:29]([O:33][CH3:34])[CH:28]=[CH:27][C:23]=1[CH2:24][CH2:25][NH2:26]>CS(C)=O>[CH3:20][O:21][C:22]1[C:30]([O:31][CH3:32])=[C:29]([O:33][CH3:34])[CH:28]=[CH:27][C:23]=1[CH2:24][CH2:25][N:26]=[C:10]([O:9][CH2:2][C:3]1[CH:4]=[CH:5][CH:6]=[CH:7][CH:8]=1)[C:15]([C:14]1[CH:13]=[CH:12][CH:11]=[CH:16][CH:18]=1)=[O:1]

Participants

4

Reactant 2

HCID 414332IsomescalineHCID 204340852-Benzyloxyphenylglyoxal hydrate

Product 1

HCID 23346555HCID 23346555, compound

Reagents, catalysts & solvents 1

HCID 679Dimethyl SulfoxideSolvent2×

Procedure

10.5 g of 2-benzyloxyphenylglyoxal hydrate (crude oil) are dissolved in 30 ml of dimethylsulfoxide, and 9 g of 2,3,4-trimethoxyphenethylamine are added thereto. The mixture is stirred at room temperature for 30 minutes, whereby a solution of α-(2,3,4-trimethoxyphenethylimino)-2-benzyloxyacetophenone in dimethylsulfoxide is obtained.

Sources & evidence

ORD record
ord-16bc5ab9c101404e87a628dd56a78919
Source dataset
uspto-grants-1980_08
Patent number
US04218479

Reaction notes

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