HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichlorobenzene → HCID 20292528, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichlorobenzene | HCID 7239 | — |
| Reactant | HCID 86737160 | HCID 86737160 | — |
| Product | HCID 20292528 | HCID 20292528 | 55% |
Reaction Steps
A mixture of diethyl-2-(1-bromoethyl)phenylphosphonate (12 g, 0.037 mole) in 25 ml. of 1,2-dichlorobenzene was refluxed for 2 hours. The reaction mixture was vacuum distilled to yield 1-ethoxy-3-methyl-1,3-dihydro-2,1-benzoxaphosphole-1-oxide (4.3 g, 55% yield) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04219510 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-d93352a1f6f442fca5275a872f531639 |
| Source note | uspto-grants-1980_08 |