反应详情

To 0.1 Mol of 1-bromo-3-methyl-4-nitro-2-butene was added 0.1 Mol of triethylphosphite. The reaction was started by immersing the mixture into a 50° C. bath and completed under continued removal of bromoethane by distillation. The residue was purified via column chromatography over silica gel using ether as solvent. The product was obtained as a yellowish liquid.

1. custominto a 50° C.
2. customcompleted under continued removal of bromoethane by distillation
3. customThe residue was purified via column chromatography over silica gel
4. customThe product was obtained as a yellowish liquid