HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichlorobenzoyl chloride → HCID 54256855, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichlorobenzoyl chloride | HCID 66645 | — |
| Reactant | 3-Methyl-4-nitrobut-2-en-1-ol | HCID 54439127 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 54256855 | HCID 54256855 | — |
Reaction Steps
To 0.1 Mol of 4-nitro-3-methyl-2-butenol in benzene was added 0.1 Mol of 2,4-dichlorobenzoylchloride and stirred overnight. The benzene was removed, the residue taken up in sat. sodiumbicarbonate solution and extracted with ether. The crude product was purified by column chromatography over silica gel using methylenechloride as eluting solvent. A yellowish oil was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04219660 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-3fb30d3a27ed4349bb02a68f5928290c |
| Source note | uspto-grants-1980_08 |