HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloride → HCID 22116874, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloride | HCID 312 | — |
| Reactant | 2,2-Dimethylsuccinic acid | HCID 11701 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Product | HCID 22116874 | HCID 22116874 | 67.8% |
Reaction Steps
2,2-Dimethylsuccinyl dichloride was prepared by reacting 2,2-dimethylsuccinic acid with PCl5 in the presence of a solvent at 20° C. After the work-up a yellow liquid was obtained which had a purity of 97.5% according to chloride content. The corrected yield was 67.8%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04219676 |
| Source dataset | uspto-grants-1980_08 |
| ORD ID | ord-55baab30041d4c5f908e755b4fbe54d2 |
| Source note | uspto-grants-1980_08 |