Sodium Azide → HCID 22132362, compound

HRID 1856655Notes

Reaction equation

[C:1]([C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[N:9]1[CH2:14][CH2:13][CH:12]([N:15]2[CH2:20][CH2:19][CH2:18][CH:17]([CH2:21]OS(CC3C=CC(C)=CC=3)(=O)=O)[CH2:16]2)[CH2:11][CH2:10]1)#[N:2].[N-:34]=[N+:35]=[N-:36].[Na+]>>[N:34]([CH2:21][CH:17]1[CH2:18][CH2:19][CH2:20][N:15]([CH:12]2[CH2:11][CH2:10][N:9]([C:4]3[CH:5]=[CH:6][CH:7]=[CH:8][C:3]=3[C:1]#[N:2])[CH2:14][CH2:13]2)[CH2:16]1)=[N+:35]=[N-:36]

Participants

Reactant 2

HCID 33557Sodium Azide

HCID 54154049HCID 54154049, compound

Product 1

HCID 22132362HCID 22132362, compound

Procedure

The title compound was prepared from 23 (1.37 g, 3.0 mmol) and sodium azide (0.4 g, 6.0 mmol) according to the procedure described in 12 to give the title compound.

Sources & evidence

ORD record: ord-752419664b594ffab38de193ec7d6afc
Source dataset: uspto-grants-2000_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06143750

Reaction notes

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