HuagongsheHuagongshe Chemistry Print Report · For research reference only
P-Anisidine → N-Methyl-m-anisidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P-Anisidine | HCID 7732 | — |
| Reactant | 3-Methoxyaniline | HCID 10824 | — |
| Product | N-Methyl-m-anisidine | HCID 84349 | 77% |
Reaction Steps
m-Anisidine (Aldrich Chemical Corp.) was substituted for p-anisidine in the procedure described in Journal Chemical Society, London, 1969:2223, Perkin Transactions I., which gave N-methyl-m-anisidine, as an oil, 24.5 g, 77% yield. NMR was consistent with structure. MS: APCI: M+1: 138.2 (M: 137.2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06143766 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-d477361a7a0141a18f3c0c674a1d7e4c |
| Source note | uspto-grants-2000_11 |