HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Ethoxy-4-ethoxycarbonylphenylacetic acid → Ethyl 2-ethoxy-4-[N-(1-(2-piperidino-phenyl)-3-methyl-1-butyl)-aminocarbonylmethyl]benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Ethoxy-4-ethoxycarbonylphenylacetic acid | HCID 10131212 | — |
| Reactant | ethyl 2-ethoxy-4-[N-{1-(2-piperidino-phenyl)-3-methyl-1-buten-1-yl}-aminocarbonylmethyl]-benzoate | HCID 53820019 | — |
| Product | Ethyl 2-ethoxy-4-[N-(1-(2-piperidino-phenyl)-3-methyl-1-butyl)-aminocarbonylmethyl]benzoate | HCID 13729227 | — |
Reaction Steps
Prepared from ethyl 2-ethoxy-4-[N-{1-(2-piperidino-phenyl)-3-methyl-1-buten-1-yl}-aminocarbonylmethyl]-benzoate, melting point 125-126° C., which in turn was prepared from (2-piperidino-phenyl)-isobutyl-ketimine and 3-ethoxy-4-ethoxycarbonyl-phenyl-acetic acid analogous to Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06143769 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-39f96604db70456abde9f3f2f0232655 |
| Source note | uspto-grants-2000_11 |