Triethylamine → HCID 178512266, compound

Participants

Reaction Steps

A solution of diphenylcyanocarbonimidate (2 mmol, 476 mg), 3,5-bis(trifluoromethyl)aniline (2 mmol, 458 mg) and triethylamine (2 mmol, 202 mg) in dichloromethane (15 ml) was stirred under nitrogen for 12 h. After concentration the residue was stirred with toluene (5 ml) for 2 h and the solid was collected by filtration giving 550 mg of N-[3,5-bis(trifluoromethyl)phenyl]-N'-cyano-O-phenylisourea (73.6%);

Provenance & Evidence