Boron tribromide → HCID 22125765, compound

HRID 1858044Notes

Reaction equation

HRID 1858044 reaction equation
[N+:1]([C:4]1[C:9]([OH:10])=[C:8]([O:11]C)[CH:7]=[C:6]([N+:13]([O-:15])=[O:14])[C:5]=1[CH2:16][CH2:17][CH2:18][CH2:19][C:20]([OH:22])=[O:21])([O-:3])=[O:2].B(Br)(Br)Br>>[OH:10][C:9]1[C:4]([N+:1]([O-:3])=[O:2])=[C:5]([CH2:16][CH2:17][CH2:18][CH2:19][C:20]([OH:22])=[O:21])[C:6]([N+:13]([O-:15])=[O:14])=[CH:7][C:8]=1[OH:11]

Participants

3

Reactant 2

HCID 25134Boron tribromideHCID 22125761HCID 22125761, compound

Product 1

HCID 22125765HCID 22125765, compound

Procedure

The product from example 5 (0.5 g) was reacted with boron tribromide according to the procedure described in example 10. Yield: 0.13 g, melting point 135-139° C.

Sources & evidence

ORD record
ord-7bee0b517897483f89e039d12d4aa6bf
Source dataset
uspto-grants-2000_11
Patent number
US06150412

Reaction notes

Loading…