HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoaniline → HCID 22125151, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoaniline | HCID 11992 | — |
| Reactant | HCID 22125053 | HCID 22125053 | — |
| Product | HCID 22125151 | HCID 22125151 | 24% |
Reaction Steps
Reaction of 4.0 g (11.1 mmol) of 5-formyl-4-[4-(tetrahydropyran-2-yloxymethyl)phenyl]amino-2-methylthiopyrimidine with 2-bromoaniline in a method analogous to Example 37(f) gave 1.13 g (24%) of 5-(2-bromoanilino)methyl-4-[4-(tetrahydropyran-2-yloxymethyl)phenyl]amino-2-methylthiopyrimidine as a pale yellow gum. [Mass spectrum (ESI) MH+ =515].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06150373 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-5e7005b7405343aab5696d533f17834e |
| Source note | uspto-grants-2000_11 |