HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Bromomethyl)benzonitrile → HCID 54139416, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Bromomethyl)benzonitrile | HCID 89599 | — |
| Reactant | tert-Butyl 3-hydroxy-4-phenylpiperidine-1-carboxylate | HCID 20664715 | — |
| Product | HCID 54139416 | HCID 54139416 | — |
Reaction Steps
In an analogous manner to that described in Example 1(g), by alkylating tert-butyl (3RS,4RS)-3-hydroxy-4-phenyl-piperidine-1-carboxylate [Example 2(a)] with 2-bromomethylbenzonitrile there was obtained tert-butyl (3RS,4RS)-3-(2-cyano-benzyloxy)-4-phenyl-piperidine-1-carboxylate as a colourless oil; MS: 393 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06150526 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-eda25d84ec154961904088f8e5e4a77d |
| Source note | uspto-grants-2000_11 |