HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylisoquinoline-5-sulfonyl chloride → HCID 70275386, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylisoquinoline-5-sulfonyl chloride | HCID 15487110 | — |
| Reactant | tert-Butyl (2S,5S)-2,5-dimethylpiperazine-1-carboxylate | HCID 24903577 | — |
| Product | HCID 70275386 | HCID 70275386 | 51.3% |
Reaction Steps
Using 0.43 g of cis-1-(tert-butoxycarbonyl)-2,5-dimethylpiperazine and 0.48 g of 5-chlorosulfonyl-4-methylisoquinoline, the procedure of Example 1 was otherwise repeated to provide 0.2 g of the objective compound (white crystals).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06153608 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-9de509a29d4f4a9bb5a050d09dabb6d3 |
| Source note | uspto-grants-2000_11 |