1-[4-(1,3-Benzodioxol-5-yl)-3-cyclohexen-1-yl]piperazine → 1-[4-(1,3-Benzodioxol-5-yl)-3-cyclohexen-1-yl]-4-[(2,5-diiodophenyl)methyl]piperazine

Participants

Reaction Steps

The title compound was prepared from 1-[4-(1,3-benzodioxol-5-yl)-3-cyclohexen-1-yl]piperazine (0.25 g, 0.87 mmole) and 2,5-diiodobenzyl chloride (0.33 g, 0.87 mmole) by the method described in example 45 to give the product (82%, mp: 174-175° C.). Calc'd for C24H26I2N2O2 : C, 45.89%; H, 4.18%; N, 4.46%. Found: C, 45.58%; H, 4.13%; N, 4.35%.

Provenance & Evidence