HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrophenylacetic acid → 2-[(3Nitrophenyl)acetamido]butyric acid iso-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrophenylacetic acid | HCID 15876 | — |
| Reactant | Isobutyl 2-aminobutyrate | HCID 13743360 | — |
| Product | 2-[(3Nitrophenyl)acetamido]butyric acid iso-butyl ester | HCID 53965912 | — |
Reaction Steps
Following General Procedure I' above and using 3-nitrophenylacetic acid (Aldrich) and iso-butyl 2-aminobutyrate (prepared following General Procedure J' above), the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by filtration as described in the general procedure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06153652 |
| Source dataset | uspto-grants-2000_11 |
| ORD ID | ord-4f01202fe39349028aa37f48771abad7 |
| Source note | uspto-grants-2000_11 |