HRID1859435

反应详情

EQUATION

反应方程式

HRID 1859435 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1.5 ml of 4 M hydrochloric acid/ethyl acetate was added to a solution of (R)-5,11-dihydro-5-[1-(3,4-methylenedioxyphenethyl) piperidine-2-ylmethyl] dibenzo [b,e][1,4] oxazepine (171 mg) in dichloromethane (5 ml), and they were stirred for 2 hours. The solvent was evaporated under reduced pressure. The title compound was obtained in the form of a white solid (150 mg, 80%).

WORKUP

后处理

  1. customThe solvent was evaporated under reduced pressure