HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphate → 2-Amino-7-isopropyl-4-methyl-benzothiazole-6-thiol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphate | HCID 1061 | — |
| Reactant | D-1,4-Dithiothreitol | HCID 446094 | — |
| Reactant | 7-Isopropyl-4-methyl-6-thiocyanato-benzothiazol-2-yl-amine | HCID 15473839 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Amino-7-isopropyl-4-methyl-benzothiazole-6-thiol | HCID 22572907 | — |
Reaction Steps
The title compound was prepared according to General Method 14 using 7-isopropyl-4-methyl-6-thiocyanato-benzothiazol-2-yl-amine (Example L-5; 11.5 g, 43.7 mmol), dithiothreitol (27.0 g, 175 mmol), EtOH (200 mL), and phosphate buffer (50 mL). MS (APCI): 239 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528510B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-d39da9417730475393ffc6d18c387612 |
| Source note | uspto-grants-2003_03 |