HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → 6-tert-Butyl-5-(toluene-4-sulfonylsulfanyl)-indole-1-carboxylic Acid Tert-Butyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Carbon Tetrachloride | HCID 5943 | — |
| Reactant | 4-Methylbenzene-1-sulfonyl bromide | HCID 10130885 | — |
| Reactant | 6-tert-Butyl-5-mercapto-indole-1-carboxylic Acid Tert-Butyl Ester | HCID 54456211 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 6-tert-Butyl-5-(toluene-4-sulfonylsulfanyl)-indole-1-carboxylic Acid Tert-Butyl Ester | HCID 54161612 | — |
Reaction Steps
The title compound was prepared according to General Method 15 using 6-tert-butyl-5-mercapto-indole-1-carboxylic acid tert-butyl ester (prepared in Example FF), pyridine, tosyl bromide, carbon tetrachloride, and EtOAc.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528510B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-f48bf30febd64c6386a5a8bde1e45cc3 |
| Source note | uspto-grants-2003_03 |