HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 4647665, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | N-(5-tert-Butyl-2-nitro-phenyl)-2,2,2-trifluoro-acetamide | HCID 22572832 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 4647665 | HCID 4647665 | — |
Reaction Steps
The title compound was prepared as outlined in Example PP-1 from N-(5-tert-butyl-2-nitro-phenyl)-2,2,2-trifluoro-acetamide (prepared in Example OO-2; 248 g, 855 mmol), MeOH (500 mL), and 7% aqueous potassium carbonate solution. The crude product was used without any purification. MS(APCI): 195 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528510B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-95e6d7c5adc54067a3ac29ba5e95c971 |
| Source note | uspto-grants-2003_03 |