HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22572976, compound → 4-tert-Butyl-5-thiocyanato-benzene-1,2-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22572976 | HCID 22572976 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Nickel | HCID 935 | — |
| Product | 4-tert-Butyl-5-thiocyanato-benzene-1,2-diamine | HCID 22572982 | — |
Reaction Steps
5-tert-Butyl-2-nitro-4-thiocyanato-phenylamine (prepared in Example QQ-2; 3 g, 12 mmol) was hydrogenated using Raney nickel (0.75 g) in the presence of hydrogen as described in General Method 3. MS(APCI): 222(M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528510B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-0b78307236ca41b7802255f21cdc18c6 |
| Source note | uspto-grants-2003_03 |