HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → 4-Tert-butyl-1-methyl-2-nitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 4-tert-Butyltoluene | HCID 7390 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4-Tert-butyl-1-methyl-2-nitrobenzene | HCID 10954415 | — |
Reaction Steps
Nitration was performed as described in General Method 12 using tert-butyl-4-methylbenzene (25 g), concentrated H2SO4 (92 g), 70% HNO3 (82 g), and H2O (25 g). The crude product was purified via distillation under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06528510B1 |
| Source dataset | uspto-grants-2003_03 |
| ORD ID | ord-5de36e6c929c4ca19e81f07725277d5a |
| Source note | uspto-grants-2003_03 |